Laboratory №8

1. Physica Modular Compact Rheometer MCR-301 - Anton Paar (Austria)
   To study the temperature-dependent visco-elastic properties of polymer solutions and melts
   
   
   
   • Viscosity determination range: 10^-2 ÷ 10⁶ Pa·s
   • Temperature range: -150 ÷ 600 °С
   • Frequency range: 10^-4 ÷ 100 Hz
   
   
2. DMA 242 C/1/F - Dynamic mechanical Analyzer - NETZSCH (Germany), 2007
   To study the temperature-dependent visco-elastic properties and determine the modulus of elasticity and the damping values by applying an oscillating force to the sample.
   
   
   Deformation modes:
   • 3-point-bending
   • single-/dual cantilever bending
   • shearing
   • compression/penetration
   • tension
   
   
   • Temperature range: -170°C ... 600°C
   • Heating and cooling rates: 0.01 K/min ... 20 K/min
   • Cooling time: 10 min (20°C ... -150°C)
   • Frequency range: 0.01 Hz ... 100 Hz
   • Modulus range (E’): 10^-3 MPa ... 10⁶ MPa
   • Damping range (tan δ): 0.00006 ... 10
   
   
3. DSC 204 F1 Phoenix® - Differential Scanning Calorimeter – NETZSCH (Germany), 2007
   For quantitative determination of the conversion temperatures and enthalpies for solids and liquids by measuring the heat flows to both the sample and to a reference as a function of temperature and time.
   
   
   
   • Temperature range: -180°C ... 700°C
   • Wide range of heating rates: 0.001 K/min ... 200 K/min
   • Fast cooling: max. 200 K/min
   
   
4. TG 209 F1 Iris® - Thermo-Microbalance – NETZSCH (Germany), 2006
   For determination of temperature- and time-dependent changes in the mass of a sample that occur during a specific temperature program and in a defined atmosphere.
   
   
   
   • Temperature range: (10) 20°C … 1000°C
   • Heating and cooling rates: 0.001 K/min … 100 K/min (temperature-dependent)
   • Cooling time: 10min (1000°C …100°C)
   • Resolution: 0.1 µg
   
   
5. DSM Xplore
   Complex of technological equipment by DSM Xplore (Netherlands) for processing of nanocomposites from the polymer melts.
   This complex includes:
   • 5 ml micro-compounder;
   • 5 ml injection molding machine;
   • micro-film device
   Maximum operating temperature - 400 °C.
   
   Pictures:
   
   
   
   
6. Universal mechanical test system UTS 10, UTStestsysteme (Germany)
   For materials mechanical tests in tension, compression, bending and shear modes, for long-term cyclic and other fatigue tests, creep and stress relaxation tests.
   
   
   
   • Temperature range: room temperature ÷ 600 °С
   • Loading range: 0.001 N ÷ 10 kN
   • Deformation speed range: 1 mcm/min ÷ 1 m/min.

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Laboratory №13

1. Diffractometer System SEIFERT XRD 3003 TT (General Electric Company)
   System supplied with highly stabilized X-Ray equipment ISO-DEBYEFLEX 3003 for structure analysis, the two circle goniometer MZ VI E in symmetrical or asymmetrical Theta / Theta configuration, scintillation counter with setting via PC compact channel board and Rayflex software.
   
   
   
   • Goniometer
   • Min. controllable step size 0.0005°
   • Reproducibility ± 0.0003°
   • Max. angle range
   • ω (tube side) = 0° - θ (detector side) = 165°
   • ω (tube side) = 165° - θ (detector side) = 0°
   
   
   • X-ray equipment ID 3003
   • Output 2 - 60 kV
   • 2 - 80 mA
   • Max. 3.5 kW,
   • ± 0.01% at ± 10% main voltage fluctuations
   
   
   
   
2. Atomic Force Microscope NT-206 (“MICROTESTMACHINES”, Belarus)
   Multifunctional scanning probe microscope NT-206 is an atomic force microscope in a complex with hardware and software enabling analysis of topography and micromechanical properties of solid surfaces with nanometre resolution.
   
   
   
   • Scanning matrix up to 512×512 points
   • Lateral resolution (plane XY): 2 nm (depending on sample hardness)
   • Vertical resolution (Z direction): 0.2÷0.4 nm (depending on sample hardness)

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